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Strontium Ferrite Disc Magnet: Example 8 Without the Orienting Field (Gorter, Philips 1956, Ex. 8 Comparison)
Charlie

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Charlie

28. 十月 2026DE
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Strontium Ferrite Disc Magnet: Example 8 Without the Orienting Field (Gorter, Philips 1956, Ex. 8 Comparison)

Made as in Example 8 but without the first, orienting field. Gorter's comparison block held 2,020 gauss with a coercive force of 3,225 oersted and a (BH)max of 0.99 × 10⁶. Source: E. W. Gorter, G. W. Rathenau and A. L. Stuyts (Philips), US 2,762,778 (1956), Example 8. They made blocks; disc size is ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
高级
3 days

说明

1

Weigh strontium carbonate and iron oxide

Weigh 29.5 g strontium carbonate and 179 g ferric oxide.

此步骤所需材料:

碳酸锶碳酸锶29.5 克
氧化铁氧化铁179 克

所需工具:

等臂天平等臂天平
P100 防毒面具P100 防毒面具
2

Mill 15 hours with alcohol, dry

Grind in a ball mill with alcohol for 15 hours. Remove the alcohol and dry the powder.

所需工具:

铁球磨机铁球磨机
乙醇——实验级,95 %乙醇——实验级,95 %
干燥炉干燥炉
3

Pre-fire 2 hours at 1000 °C in air

Heat the powder for 2 hours at 1000 °C in an electric furnace in air. Let it cool.

所需工具:

马弗炉马弗炉
带盖坩埚(瓷质)带盖坩埚(瓷质)
坩埚钳坩埚钳
耐热手套耐热手套
4

Grind 4 hours in an agate centrifugal mill

Grind the cooled material for 4 hours with alcohol in an agate centrifugal mill, then dry it. This is the pre-fired powder.

所需工具:

玛瑙离心研磨机玛瑙离心研磨机
乙醇——实验级,95 %乙醇——实验级,95 %
干燥炉干燥炉
5

Stir into 8 % polyvinyl acetate in acetone

Dissolve polyvinyl acetate in acetone to a 8 % solution and stir the pre-fired powder into it, 1 cc of solution per gram of powder. The binder burns off later.

所需工具:

聚乙酸乙烯酯聚乙酸乙烯酯
丙酮丙酮
等臂天平等臂天平
6

Mould without a first field

Put the suspension in a moulding die and remove the binder solution without any magnetic field. This is the patent's comparison block.

所需工具:

圆片压模圆片压模
液压机液压机
7

Heat to 500 °C in a 2000 oersted field

Put the block in an electric furnace between the magnet's poles. With a second field of 2000 oersted along the first field's direction, heat to 500 °C, which burns off the rest of the binder. Then switch the field off.

所需工具:

管式炉管式炉
电磁铁电磁铁
耐热手套耐热手套
8

Sinter: through a 1280 °C zone in 5 minutes

Pass the block at 20 mm per minute through an electric furnace in air at 1280 °C with a 10 cm hot zone: about 5 minutes in the heat.

所需工具:

管式炉管式炉
耐热手套耐热手套
9

Magnetise the block

Magnetise the block in a field. Without the orienting field it has no preferred direction. Ours: an electromagnet. Find the north face with a compass.

所需工具:

电磁铁电磁铁
指南针指南针

材料

2

所需工具

17

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