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Strontium Ferrite Disc Magnet: 0.7 mol SrCO3 to 3.2 mol Iron Oxide, 1280 °C (Went, Philips 1956, Ex. 12)
A strontium ferrite: 0.7 mol strontium carbonate to 3.2 mol iron oxide, milled, bound and formed as in Example 4, and passed through a 1280 °C furnace in 10 minutes. Went's rod held 1,955 gauss with a coercive force of 2,900 oersted.
Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 12. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
高级
2 days
说明
1
1
Weigh strontium carbonate and iron oxide
Weigh strontium carbonate and iron oxide
Weigh 103.3 g strontium carbonate (0.7 mol) and 503.0 g ferric oxide (3.2 mol).
此步骤所需材料：
碳酸锶103.3 克
氧化铁503 克所需工具：
等臂天平
P100 防毒面具2
2
Mill with alcohol 15.5 hours, dry and sieve
Mill with alcohol 15.5 hours, dry and sieve
As in Example 4: grind the mixture with alcohol in a ball mill for 15.5 hours, then dry it and sieve it.
所需工具：
铁球磨机
乙醇——实验级，95 %
干燥炉
粗筛3
3
Knead with a binder and form
Knead with a binder and form
Mix 300 g of the powder with a binder such as polyvinyl alcohol (Went names it or nitrocellulose) into a kneadable mass. The patent extrudes rods about 3 mm across; ours: press discs at 1.5 tonnes per cm², as in its other examples. Dry them in air for about 24 hours.
所需工具：
聚乙烯醇粉末
液压机
圆片压模干燥炉4
4
Pass through a 1280 °C zone in 10 minutes
Pass through a 1280 °C zone in 10 minutes
Sinter in air at 1280 °C by passing the pieces through a 10 cm hot zone at 10 mm per minute: 10 minutes in the heat.
所需工具：
管式炉
耐热手套5
5
Magnetise the discs
Magnetise the discs
The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.
所需工具：
电磁铁
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