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Hydrogen Peroxide 3 %: Barium Peroxide in Dilute Sulphuric Acid
Thénard first made hydrogen peroxide from barium peroxide; the improved way stirs the peroxide into sulphuric acid, which takes the barium out as insoluble barium sulphate. Titrate the clear liquid with permanganate to find its strength, dilute it to 3 %, the mild antiseptic and bleach, and keep it in a dark bottle. Even 3 % hurts the eyes.
The picture: our diagram of the four stages.
Juu
A day
Maagizo
1
1
Peroxide into cold acid
Peroxide into cold acid
Grind the barium peroxide to a paste with a little cold water. Stand a beaker of dilute sulphuric acid in ice and stir the paste in a little at a time. Stop while a drop of the liquid still turns blue litmus red: it keeps better slightly acid.
Vifaa kwa hatua hii:
Peroksidi ya bariamu150 g
Asidi ya sulfuriki iliyopunguzwa1 litaZana zinazohitajika:
Kinu na mchi
Mizani ya mizani-mbili
Bikari ya Borosilikati
Sufuria Kubwa
Vipande vya barafu
Fimbo ya Kioo ya Kukoroga
Karatasi ya litmasi
Miwani ya kinga dhidi ya kemikali
Glavu za mpira2
2
Filter
Filter
Let the white barium sulphate settle and filter it off. The clear liquid is hydrogen peroxide in water.
Zana zinazohitajika:
Faneli ya Kioo Yenye Bomba
Karatasi ya Kuchuja
Bikari ya Borosilikati
Miwani ya kinga dhidi ya kemikali
Glavu za mpira3
3
Titrate a sample
Titrate a sample
Dissolve 3.161 g of permanganate to 1 litre in a volumetric flask. Pipette 1 mL of the peroxide into a flask with some dilute sulphuric acid and run permanganate in from the burette until the first lasting pink. Note the reading (step 5).
Zana zinazohitajika:
Pamanganati ya potasiamu — KMnO4
Chupa ya ujazo
Pipeti iliyodarajwa (ya Mohr)
Chupa ya Erlenmeyer
Bureti (ya kioo)
Kibano cha maabara (bureti/chupa)
Asidi ya sulfuriki iliyopunguzwa
Miwani ya kinga dhidi ya kemikali
Glavu za mpira4
4
Dilute and bottle
Dilute and bottle
Weigh the batch, stir in the distilled water the notebook gives, and keep it cool in a dark, closed bottle.
Vifaa kwa hatua hii:
Maji yaliyosafishwa kwa mvuke0.1 litaZana zinazohitajika:
Mizani ya mizani-mbili
Fimbo ya Kioo ya Kukoroga
Chupa ya kioo cha kahawia
Miwani ya kinga dhidi ya kemikali
Glavu za mpira5
5
Strength and dilution
Strength and dilution
Inapakia daftari la Jupyter…
Vifaa
3- 150 gKishikilia Nafasi
- Kishikilia Nafasi
- 0.1 litaKishikilia Nafasi
Zana Zinazohitajika
19- Kishikilia Nafasi
- Kishikilia Nafasi
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- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
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