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Potassium Permanganate: Pyrolusite Fused with Caustic Potash, Turned Purple by Carbonic Acid
Glauber fused pyrolusite with potash in 1659 and watched the solution turn from green to violet to red: the chemical chameleon. Fuse the ore with caustic potash and saltpetre to green potassium manganate, then bubble carbonic acid through its solution to make purple permanganate. It is a strong oxidiser: keep it away from paper, wood and oil.
The picture: potassium permanganate crystals.
Juu
Two days
Maagizo
1
1
Grind and weigh
Grind and weigh
Grind the pyrolusite fine and sift it. Weigh out caustic potash and saltpetre for it (step 6).
Vifaa kwa hatua hii:
Madini ya piroluziti (dayoksidi ya manganizi)100 g
Hidroksidi ya potasiamu130 gZana zinazohitajika:
Nitrati ya potasiamu (chumvi ya baruti)
Kinu na mchi
Ungo wa Matundu Membamba
Mizani ya mizani-mbili
Miwani ya kinga dhidi ya kemikali
Glavu za mpira2
2
Fuse
Fuse
Melt the caustic potash in an iron crucible in the furnace and stir in the ore and saltpetre a little at a time with an iron rod. Keep it hot, stirring, until the mass is dark green. Lift it out and let it cool.
Zana zinazohitajika:
Kalibu ya chuma
Tanuru la mkaa
Mkaa
Fimbo ya chuma
Koleo la kaure ya kuyeyushia
Glavu za kulehemu
Miwani ya kinga dhidi ya kemikali3
3
Dissolve the green salt
Dissolve the green salt
Break up the cold melt and dissolve it in water. The solution is green.
Vifaa kwa hatua hii:
Maji yaliyosafishwa kwa mvuke1 litaZana zinazohitajika:
Bikari ya Borosilikati
Fimbo ya Kioo ya Kukoroga
Miwani ya kinga dhidi ya kemikali
Glavu za mpira4
4
Turn it purple
Turn it purple
Bubble carbon dioxide through the solution from a glass tube until it turns deep purple and brown manganese dioxide settles out.
Zana zinazohitajika:
Gesi ya kaboni dioksidi
Seti ya Mirija ya Kioo
Bikari ya Borosilikati
Miwani ya kinga dhidi ya kemikali
Glavu za mpira5
5
Crystallise
Crystallise
Let the brown sludge settle and pour the clear purple liquid off it; do not filter through paper, which it attacks. Evaporate on the sand bath until crystals form on cooling. Drain the dark purple needles and keep them in a closed glass jar.
Zana zinazohitajika:
Sahani ya Kuvukizia
Bafu la mchanga
Chupa ya Kioo
Miwani ya kinga dhidi ya kemikali
Glavu za mpira6
6
Charge and yield
Charge and yield
Inapakia daftari la Jupyter…
Vifaa
3- Kishikilia Nafasi
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Zana Zinazohitajika
19- Kishikilia Nafasi
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Mchoro huu unatengeneza
Blueprint zinazohusiana
Blueprint hizi zinashiriki maarifa — mbinu, vifaa au kanuni
CC0 Umma Wote
Mchoro huu umetolewa chini ya CC0. Uko huru kunakili, kubadilisha, kusambaza, na kutumia kazi hii kwa madhumuni yoyote, bila kuomba ruhusa.
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