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PTFE Disc: Sintered in a Molten Nitrate Bath, Cooled Slowly (Brubaker & Hanford 1946)
Emma

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Emma

27. Oktoba 2026SE
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PTFE Disc: Sintered in a Molten Nitrate Bath, Cooled Slowly (Brubaker & Hanford 1946)

A PTFE disc pressed cold, then sintered by dipping it in molten salt at 380 °C for half an hour. Instead of being quenched, it cools slowly between magnesite blocks. The patent says slowly cooled pieces are a little softer and less stiff, which is often better for machining. Source: M. M. Brubaker and W. E. Hanford (du Pont), US 2,400,099 (1946), Example II. The patent gives no nitrate-to-nitrite ratio. The mould, press, pot and burner are ours. Picture drawn by Youblob.
Juu
1 day

Maagizo

1

Press a disc at 500 psi

At 25 °C, press PTFE powder at 500 lb/sq in into a disc 2 in across and ⅜ in thick.

Vifaa kwa hatua hii:

Unga wa resini ya PTFEUnga wa resini ya PTFE1 as required for the disc

Zana zinazohitajika:

Kalibu ya kubanaKalibu ya kubana
Mashine ya kubana ya haidrolikiMashine ya kubana ya haidroliki
RulaRula
2

Melt the salt bath at 380 °C

Melt a mixture of sodium nitrate and sodium nitrite and hold it at 380 °C. The patent gives no ratio. Ours: a cast iron pot on a gas burner.

Zana zinazohitajika:

Chumvi ya baruti ya Chile (nitrati ya sodiamu)Chumvi ya baruti ya Chile (nitrati ya sodiamu)
Nitriti ya sodiamuNitriti ya sodiamu
Chungu cha chuma cha kutupwaChungu cha chuma cha kutupwa
Kichomea cha gesiKichomea cha gesi
Themokapo yenye kionyeshiThemokapo yenye kionyeshi
3

Dip the disc for half an hour

Lower the pressed disc into the molten bath and leave it there for ½ hour.

Zana zinazohitajika:

KoleoKoleo
Chungu cha chuma cha kutupwaChungu cha chuma cha kutupwa
Themokapo yenye kionyeshiThemokapo yenye kionyeshi
4

Cool it slowly between magnesite blocks

Take the disc out and lay it between two magnesite blocks so it cools to room temperature over 1 hour. It comes out tough and even, close to its pressed shape.

Zana zinazohitajika:

KoleoKoleo
Matofali ya magnesitiMatofali ya magnesiti

Vifaa

1

Zana Zinazohitajika

10

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