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Violet Iron Oxide: Precipitated Hematite Calcined at 1000-1100 °C (Nurdini et al. 2022)
Iron hydroxide is thrown down from hot ferric nitrate solution with ammonia, washed, dried and calcined. All of it ends as pure hematite, but the colour moves from bright red through dark red to purple as the calcining heat rises from 1000 °C, because the grains grow larger and more crystalline.
Result: pure violet to purple ferric oxide (hematite) after 4 hours at 1000-1100 °C.
Source: Nurdini et al., Heliyon 8 (2022) e10377, sections 2.2 and 4. Not given: batch size, how much ammonia, end pH, yield. Picture drawn by Youblob.
Kati
2 days
Maagizo
1
1
Heat the ferric nitrate solution
Heat the ferric nitrate solution
Make a 0.05 M solution of ferric nitrate in distilled water and heat it to 80 °C.
Vifaa kwa hatua hii:
Nitrati ya feri1 as requiredZana zinazohitajika:
Maji yaliyosafishwa kwa mvuke
Bikari ya kioo
Sahani ya Kupasha Joto
Kipimajoto2
2
Throw down the hydroxide with ammonia
Throw down the hydroxide with ammonia
Keeping it at 80 °C, add ammonia solution drop by drop while stirring well. Stir for 3 hours, then let it cool to room temperature: a red-brown precipitate forms. Not given: how much ammonia.
Zana zinazohitajika:
Myeyusho wa amonia - asilimia 25-28
Funeli ya kudondoshaSahani ya Kupasha JotoKipimajoto3
3
Spin down, wash and dry
Spin down, wash and dry
Collect the precipitate in a centrifuge at 4000 rpm for 15 minutes, wash it with distilled water, and dry it at 110 °C for 24 hours.
Zana zinazohitajika:
Kizungushi cha mezaMaji yaliyosafishwa kwa mvuke
Tanuri la kukaushia4
4
Calcine at 1000-1100 °C
Calcine at 1000-1100 °C
Calcine for 4 hours in air at 1000-1100 °C. Below 1000 °C it stays bright or dark red; from 1000 °C it turns purple. Grind the cooled oxide to a fine powder (they used an agate mortar).
Zana zinazohitajika:
Tanuri ya muffle
Kinu na mchiVifaa
1- 1 as requiredKishikilia Nafasi
Zana Zinazohitajika
10- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
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- Kishikilia Nafasi
- Kishikilia Nafasi
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