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Barium-Calcium Ferrite Disc Magnet: Part of the Barium Replaced by Calcium (Went, Philips 1956, Ex. 21)
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28. Oṣù Kẹwà 2026DE
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Barium-Calcium Ferrite Disc Magnet: Part of the Barium Replaced by Calcium (Went, Philips 1956, Ex. 21)

A ceramic magnet in which part of the barium is replaced by calcium: 0.06 mol barium carbonate and 0.04 mol calcium carbonate to 0.6 mol iron oxide, milled, fired in oxygen, milled again, pressed and passed quickly through a hot furnace. Went's rod held 1,660 gauss with a coercive force of 1,210 oersted. Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 21. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Ilọsíwájú
2 days

Ìlànà

1

Weigh barium carbonate, chalk and iron oxide

Weigh 11.84 g barium carbonate (0.06 mol), 4.004 g calcium carbonate (0.04 mol) and 99.55 g ferric oxide (0.6 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.

Àwọn ohun èlò fún ìgbésẹ̀ yìí:

Barium carbonate (witherite)Barium carbonate (witherite)11.84 g
Calcium carbonate (ẹfun funfun)Calcium carbonate (ẹfun funfun)4.004 g
Ọ́kísáìdì irin (III)Ọ́kísáìdì irin (III)99.55 g

Àwọn irinṣẹ́ tí a nílò:

Òǹwọ̀n ìdọ́gbaÒǹwọ̀n ìdọ́gba
Ìbọ̀wọ́ rọ́bàÌbọ̀wọ́ rọ́bà
Ẹ̀rọ Ìmí P100Ẹ̀rọ Ìmí P100
2

Mill with alcohol 4 hours and dry

Grind the mixture with alcohol in a ball mill for 4 hours, then dry it.

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀rọ Lílọ Bọ́ọ̀lù IrinẸ̀rọ Lílọ Bọ́ọ̀lù Irin
Ethanol - ìpele ilé-ìwádìí, 95 %Ethanol - ìpele ilé-ìwádìí, 95 %
Ààrò ìgbẹ̀Ààrò ìgbẹ̀
3

Presinter in oxygen at 1000 °C for 2 hours

Fire the dry powder in oxygen at 1000 °C for 2 hours (ours: a tube furnace fed from an oxygen cylinder).

Àwọn irinṣẹ́ tí a nílò:

Ààrò Ọ̀pọ́nÀàrò Ọ̀pọ́n
OxygenOxygen
Àgbá gáàsì tí a fi ìfúnpá kúnÀgbá gáàsì tí a fi ìfúnpá kún
Ìbọ̀wọ́ Tí Ń Fara Da OoruÌbọ̀wọ́ Tí Ń Fara Da Ooru
4

Mill again 4 hours, dry, press at 1.5 t/cm²

Grind with alcohol in the ball mill for 4 hours, dry, and press at 1.5 tonnes per cm² (ours: discs instead of rods).

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀rọ Lílọ Bọ́ọ̀lù IrinẸ̀rọ Lílọ Bọ́ọ̀lù Irin
Ethanol - ìpele ilé-ìwádìí, 95 %Ethanol - ìpele ilé-ìwádìí, 95 %
Ààrò ìgbẹ̀Ààrò ìgbẹ̀
Ẹ̀rọ ìtẹ̀ háídírọ́líìkìẸ̀rọ ìtẹ̀ háídírọ́líìkì
Mọ́ọ̀dù títẹ díìsìMọ́ọ̀dù títẹ díìsì
5

Pass through a 1200 °C zone in 10 minutes

Sinter at 1200 °C by passing the pieces through a 10 cm hot zone at 10 mm per minute, which is 10 minutes in the heat.

Àwọn irinṣẹ́ tí a nílò:

Ààrò Ọ̀pọ́nÀàrò Ọ̀pọ́n
Ìbọ̀wọ́ Tí Ń Fara Da OoruÌbọ̀wọ́ Tí Ń Fara Da Ooru
6

Magnetise the discs

The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.

Àwọn irinṣẹ́ tí a nílò:

Òòfà iná-mànàmánáÒòfà iná-mànàmáná
Kọ́mpasiKọ́mpasi

Àwọn ohun-èlò

3

Àwọn irinṣẹ́ tó nílò

14

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