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Barium-Calcium Ferrite Disc Magnet: Equal Barium and Calcium, Sintered at 1280 °C (Went, Philips 1956, Ex. 22)
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28. Oṣù Kẹwà 2026DE
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Barium-Calcium Ferrite Disc Magnet: Equal Barium and Calcium, Sintered at 1280 °C (Went, Philips 1956, Ex. 22)

A ceramic magnet with equal parts barium and calcium: 0.3 mol barium carbonate, 0.3 mol calcium carbonate and 3.1 mol iron oxide, milled 15 hours, pressed and passed through a 1280 °C furnace in 10 minutes, with no presintering. Went's rod held 1,595 gauss with a coercive force of 1,890 oersted. Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 22. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Ilọsíwájú
2 days

Ìlànà

1

Weigh barium carbonate, chalk and iron oxide

Weigh 59.5 g barium carbonate (0.3 mol), 30.2 g calcium carbonate (0.3 mol) and 500.0 g ferric oxide (3.1 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.

Àwọn ohun èlò fún ìgbésẹ̀ yìí:

Barium carbonate (witherite)Barium carbonate (witherite)59.5 g
Calcium carbonate (ẹfun funfun)Calcium carbonate (ẹfun funfun)30.2 g
Ọ́kísáìdì irin (III)Ọ́kísáìdì irin (III)500 g

Àwọn irinṣẹ́ tí a nílò:

Òǹwọ̀n ìdọ́gbaÒǹwọ̀n ìdọ́gba
Ìbọ̀wọ́ rọ́bàÌbọ̀wọ́ rọ́bà
Ẹ̀rọ Ìmí P100Ẹ̀rọ Ìmí P100
2

Mill with alcohol 15 hours, dry, press

Grind with alcohol in a ball mill for 15 hours, dry, and press at 1.5 tonnes per cm² (ours: discs instead of rods). No presintering.

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀rọ Lílọ Bọ́ọ̀lù IrinẸ̀rọ Lílọ Bọ́ọ̀lù Irin
Ethanol - ìpele ilé-ìwádìí, 95 %Ethanol - ìpele ilé-ìwádìí, 95 %
Ààrò ìgbẹ̀Ààrò ìgbẹ̀
Ẹ̀rọ ìtẹ̀ háídírọ́líìkìẸ̀rọ ìtẹ̀ háídírọ́líìkì
Mọ́ọ̀dù títẹ díìsìMọ́ọ̀dù títẹ díìsì
3

Pass through a 1280 °C zone in 10 minutes

Sinter at 1280 °C by passing the pieces through a 10 cm hot zone at 10 mm per minute: 10 minutes in the heat.

Àwọn irinṣẹ́ tí a nílò:

Ààrò Ọ̀pọ́nÀàrò Ọ̀pọ́n
Ìbọ̀wọ́ Tí Ń Fara Da OoruÌbọ̀wọ́ Tí Ń Fara Da Ooru
4

Magnetise the discs

The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.

Àwọn irinṣẹ́ tí a nílò:

Òòfà iná-mànàmánáÒòfà iná-mànàmáná
Kọ́mpasiKọ́mpasi

Àwọn ohun-èlò

3

Àwọn irinṣẹ́ tó nílò

12

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