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Barium Ferrite Disc Magnet: 1 mol BaCO3 to 2.5 mol Iron Oxide, 1310 °C (Went, Philips 1956, Ex. 1)
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Barium Ferrite Disc Magnet: 1 mol BaCO3 to 2.5 mol Iron Oxide, 1310 °C (Went, Philips 1956, Ex. 1)

Went's first barium ferrite: 1 mol barium carbonate to 2.5 mol iron oxide, milled 13.5 hours, bound, formed and passed through a 1310 °C furnace in 20 minutes. His rod held 1,200 gauss with a coercive force of 1,940 oersted. Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 1. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Ilọsíwájú
2 days

Ìlànà

1

Weigh barium carbonate and iron oxide

Weigh 201.1 g barium carbonate (1 mol) and 400.5 g ferric oxide (2.5 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.

Àwọn ohun èlò fún ìgbésẹ̀ yìí:

Barium carbonate (witherite)Barium carbonate (witherite)201.1 g
Ọ́kísáìdì irin (III)Ọ́kísáìdì irin (III)400.5 g

Àwọn irinṣẹ́ tí a nílò:

Òǹwọ̀n ìdọ́gbaÒǹwọ̀n ìdọ́gba
Ìbọ̀wọ́ rọ́bàÌbọ̀wọ́ rọ́bà
Ẹ̀rọ Ìmí P100Ẹ̀rọ Ìmí P100
2

Mill with alcohol 13.5 hours, dry and sieve

Grind the mixture with alcohol in a ball mill for 13.5 hours, then dry it and sieve it.

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀rọ Lílọ Bọ́ọ̀lù IrinẸ̀rọ Lílọ Bọ́ọ̀lù Irin
Ethanol - ìpele ilé-ìwádìí, 95 %Ethanol - ìpele ilé-ìwádìí, 95 %
Ààrò ìgbẹ̀Ààrò ìgbẹ̀
Ajọ̀Ajọ̀
3

Knead with a binder and form

Mix 300 g of the powder with a binder such as polyvinyl alcohol (Went names it or nitrocellulose) into a kneadable mass. The patent extrudes rods about 3 mm across; ours: press discs at 1.5 tonnes per cm², as in its other examples. Dry them in air for about 24 hours.

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀lúbọ́ polyvinyl alcoholẸ̀lúbọ́ polyvinyl alcohol
Ẹ̀rọ ìtẹ̀ háídírọ́líìkìẸ̀rọ ìtẹ̀ háídírọ́líìkì
Mọ́ọ̀dù títẹ díìsìMọ́ọ̀dù títẹ díìsì
Ààrò ìgbẹ̀Ààrò ìgbẹ̀
4

Pass through a 1310 °C zone in 20 minutes

Sinter in air at 1310 °C by passing the pieces through a 10 cm hot zone at 5 mm per minute: 20 minutes in the heat.

Àwọn irinṣẹ́ tí a nílò:

Ààrò Ọ̀pọ́nÀàrò Ọ̀pọ́n
Ìbọ̀wọ́ Tí Ń Fara Da OoruÌbọ̀wọ́ Tí Ń Fara Da Ooru
5

Magnetise the discs

The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.

Àwọn irinṣẹ́ tí a nílò:

Òòfà iná-mànàmánáÒòfà iná-mànàmáná
Kọ́mpasiKọ́mpasi

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