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Barium-Strontium Ferrite Disc Magnet: 0.5 mol BaCO3, 0.5 mol SrCO3, 1240 °C (Went, Philips 1956, Ex. 29)
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Barium-Strontium Ferrite Disc Magnet: 0.5 mol BaCO3, 0.5 mol SrCO3, 1240 °C (Went, Philips 1956, Ex. 29)

A ceramic magnet with both barium and strontium: 0.5 mol barium carbonate and 0.5 mol strontium carbonate to 2.5 mol iron oxide, milled as in Example 28, pressed and passed through a 1240 °C furnace in 10 minutes. Went's rod held 1,550 gauss with a coercive force of 3,410 oersted. Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 29. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Ilọsíwájú
2 days

Ìlànà

1

Weigh the carbonates and iron oxide

Weigh 99.2 g barium carbonate (0.5 mol), 73.8 g strontium carbonate (0.5 mol), 402.0 g ferric oxide (2.5 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.

Àwọn ohun èlò fún ìgbésẹ̀ yìí:

Barium carbonate (witherite)Barium carbonate (witherite)99.2 g
Strontium carbonateStrontium carbonate73.8 g
Ọ́kísáìdì irin (III)Ọ́kísáìdì irin (III)402 g

Àwọn irinṣẹ́ tí a nílò:

Òǹwọ̀n ìdọ́gbaÒǹwọ̀n ìdọ́gba
Ìbọ̀wọ́ rọ́bàÌbọ̀wọ́ rọ́bà
Ẹ̀rọ Ìmí P100Ẹ̀rọ Ìmí P100
2

Mill with alcohol 15 hours, dry

As in Example 28: grind the mixture with alcohol in a ball mill for 15 hours, then dry it.

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀rọ Lílọ Bọ́ọ̀lù IrinẸ̀rọ Lílọ Bọ́ọ̀lù Irin
Ethanol - ìpele ilé-ìwádìí, 95 %Ethanol - ìpele ilé-ìwádìí, 95 %
Ààrò ìgbẹ̀Ààrò ìgbẹ̀
3

Press the powder

Example 28 moulds a rod without giving the pressure. Ours: press discs at 1.5 tonnes per cm², the pressure of the patent's other examples.

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀rọ ìtẹ̀ háídírọ́líìkìẸ̀rọ ìtẹ̀ háídírọ́líìkì
Mọ́ọ̀dù títẹ díìsìMọ́ọ̀dù títẹ díìsì
4

Pass through a 1240 °C zone in 10 minutes

Sinter at 1240 °C by passing the pieces through a 10 cm hot zone at 10 mm per minute: 10 minutes in the heat.

Àwọn irinṣẹ́ tí a nílò:

Ààrò Ọ̀pọ́nÀàrò Ọ̀pọ́n
Ìbọ̀wọ́ Tí Ń Fara Da OoruÌbọ̀wọ́ Tí Ń Fara Da Ooru
5

Magnetise the discs

The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.

Àwọn irinṣẹ́ tí a nílò:

Òòfà iná-mànàmánáÒòfà iná-mànàmáná
Kọ́mpasiKọ́mpasi

Àwọn ohun-èlò

3

Àwọn irinṣẹ́ tó nílò

12

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