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PTFE Disc: Sintered in a Molten Nitrate Bath, Cooled Slowly (Brubaker & Hanford 1946)
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PTFE Disc: Sintered in a Molten Nitrate Bath, Cooled Slowly (Brubaker & Hanford 1946)

A PTFE disc pressed cold, then sintered by dipping it in molten salt at 380 °C for half an hour. Instead of being quenched, it cools slowly between magnesite blocks. The patent says slowly cooled pieces are a little softer and less stiff, which is often better for machining. Source: M. M. Brubaker and W. E. Hanford (du Pont), US 2,400,099 (1946), Example II. The patent gives no nitrate-to-nitrite ratio. The mould, press, pot and burner are ours. Picture drawn by Youblob.
Ilọsíwájú
1 day

Ìlànà

1

Press a disc at 500 psi

At 25 °C, press PTFE powder at 500 lb/sq in into a disc 2 in across and ⅜ in thick.

Àwọn ohun èlò fún ìgbésẹ̀ yìí:

Erùpẹ̀ resini PTFEErùpẹ̀ resini PTFE1 as required for the disc

Àwọn irinṣẹ́ tí a nílò:

Àwòṣe ìtẹ̀mọ́lẹ̀Àwòṣe ìtẹ̀mọ́lẹ̀
Ẹ̀rọ ìtẹ̀ háídírọ́líìkìẸ̀rọ ìtẹ̀ háídírọ́líìkì
Ìdíwọ̀nÌdíwọ̀n
2

Melt the salt bath at 380 °C

Melt a mixture of sodium nitrate and sodium nitrite and hold it at 380 °C. The patent gives no ratio. Ours: a cast iron pot on a gas burner.

Àwọn irinṣẹ́ tí a nílò:

Iyọ̀ ìbọn Chile (sodium nitrate)Iyọ̀ ìbọn Chile (sodium nitrate)
Sodium nitriteSodium nitrite
Ìkòkò irin dídàÌkòkò irin dídà
Ohun ìdáná gáàsìOhun ìdáná gáàsì
Thermocouple pẹ̀lú ìkàThermocouple pẹ̀lú ìkà
3

Dip the disc for half an hour

Lower the pressed disc into the molten bath and leave it there for ½ hour.

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀múẸ̀mú
Ìkòkò irin dídàÌkòkò irin dídà
Thermocouple pẹ̀lú ìkàThermocouple pẹ̀lú ìkà
4

Cool it slowly between magnesite blocks

Take the disc out and lay it between two magnesite blocks so it cools to room temperature over 1 hour. It comes out tough and even, close to its pressed shape.

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀múẸ̀mú
Búlọ́ọ̀kù magnesiteBúlọ́ọ̀kù magnesite

Àwọn ohun-èlò

1

Àwọn irinṣẹ́ tó nílò

10

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