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PTFE Disc: Sintered in a Molten Nitrate Bath, Cooled Slowly (Brubaker & Hanford 1946)
A PTFE disc pressed cold, then sintered by dipping it in molten salt at 380 °C for half an hour. Instead of being quenched, it cools slowly between magnesite blocks. The patent says slowly cooled pieces are a little softer and less stiff, which is often better for machining.
Source: M. M. Brubaker and W. E. Hanford (du Pont), US 2,400,099 (1946), Example II. The patent gives no nitrate-to-nitrite ratio. The mould, press, pot and burner are ours. Picture drawn by Youblob.
Ilọsíwájú
1 day
Ìlànà
1
1
Press a disc at 500 psi
Press a disc at 500 psi
At 25 °C, press PTFE powder at 500 lb/sq in into a disc 2 in across and ⅜ in thick.
Àwọn ohun èlò fún ìgbésẹ̀ yìí:
Erùpẹ̀ resini PTFE1 as required for the discÀwọn irinṣẹ́ tí a nílò:
Àwòṣe ìtẹ̀mọ́lẹ̀
Ẹ̀rọ ìtẹ̀ háídírọ́líìkì
Ìdíwọ̀n2
2
Melt the salt bath at 380 °C
Melt the salt bath at 380 °C
Melt a mixture of sodium nitrate and sodium nitrite and hold it at 380 °C. The patent gives no ratio. Ours: a cast iron pot on a gas burner.
Àwọn irinṣẹ́ tí a nílò:
Iyọ̀ ìbọn Chile (sodium nitrate)
Sodium nitrite
Ìkòkò irin dídà
Ohun ìdáná gáàsì
Thermocouple pẹ̀lú ìkà3
3
Dip the disc for half an hour
Dip the disc for half an hour
Lower the pressed disc into the molten bath and leave it there for ½ hour.
Àwọn irinṣẹ́ tí a nílò:
Ẹ̀mú
Ìkòkò irin dídà
Thermocouple pẹ̀lú ìkà4
4
Cool it slowly between magnesite blocks
Cool it slowly between magnesite blocks
Take the disc out and lay it between two magnesite blocks so it cools to room temperature over 1 hour. It comes out tough and even, close to its pressed shape.
Àwọn irinṣẹ́ tí a nílò:
Ẹ̀mú
Búlọ́ọ̀kù magnesiteÀwọn ohun-èlò
1- 1 as required for the discÀyè
Àwọn irinṣẹ́ tó nílò
10- Àyè
- Àyè
Ìtọ́nisọ́nà yìí ń ṣe
Blueprint tó jọra
Àwọn blueprint wọ̀nyí pín ìmọ̀ — ọ̀nà, ohun-èlò tàbí ìlànà

PTFE Resin Powder: Tetrafluoroethylene Polymerised under Pressure, Plunkett 1941
láti ọwọ́ Charlie
Ti Ilé-iṣẹ́
5
0
0
0
0
0

PTFE Ring: Pressed Cold, Sintered Out of the Mould (Brubaker & Hanford 1946)
láti ọwọ́ Emma
Iṣẹ́ Ṣílíìkì
13
0
0
0
0
0

PTFE Rod: a Plug Sintered in Boiling Retene Vapour (Brubaker & Hanford 1946)
láti ọwọ́ Emma
Iṣẹ́ Ṣílíìkì
9
0
0
0
0
0
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