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Strontium-Calcium Ferrite Disc Magnet: 0.08 mol SrCO3 and 0.02 mol CaCO3, 1280 °C (Went, Philips 1956, Ex. 23)
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Strontium-Calcium Ferrite Disc Magnet: 0.08 mol SrCO3 and 0.02 mol CaCO3, 1280 °C (Went, Philips 1956, Ex. 23)

A strontium ferrite with a fifth of the strontium replaced by calcium: 0.08 mol strontium carbonate and 0.02 mol calcium carbonate to 0.6 mol iron oxide, ground, dried, formed and passed through a 1280 °C furnace in 10 minutes. Went's rod held 2,320 gauss with a coercive force of 1,395 oersted. Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 23. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Ilọsíwájú
2 days

Ìlànà

1

Weigh the carbonates and iron oxide

Weigh 11.81 g strontium carbonate (0.08 mol), 2.002 g calcium carbonate (0.02 mol), 95.55 g ferric oxide (0.6 mol).

Àwọn ohun èlò fún ìgbésẹ̀ yìí:

Strontium carbonateStrontium carbonate11.81 g
Calcium carbonate (ẹfun funfun)Calcium carbonate (ẹfun funfun)2.002 g
Ọ́kísáìdì irin (III)Ọ́kísáìdì irin (III)95.55 g

Àwọn irinṣẹ́ tí a nílò:

Òǹwọ̀n ìdọ́gbaÒǹwọ̀n ìdọ́gba
Ẹ̀rọ Ìmí P100Ẹ̀rọ Ìmí P100
2

Mill with alcohol 4 hours, dry

As in Examples 18 to 21: grind the mixture with alcohol in a ball mill for 4 hours, then dry it.

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀rọ Lílọ Bọ́ọ̀lù IrinẸ̀rọ Lílọ Bọ́ọ̀lù Irin
Ethanol - ìpele ilé-ìwádìí, 95 %Ethanol - ìpele ilé-ìwádìí, 95 %
Ààrò ìgbẹ̀Ààrò ìgbẹ̀
3

Press at 1.5 t/cm²

Example 23 does not say whether the 1000 °C presinter of Examples 18 to 21 is used. Press the dry powder at 1.5 tonnes per cm² (ours: discs instead of a rod).

Àwọn irinṣẹ́ tí a nílò:

Ẹ̀rọ ìtẹ̀ háídírọ́líìkìẸ̀rọ ìtẹ̀ háídírọ́líìkì
Mọ́ọ̀dù títẹ díìsìMọ́ọ̀dù títẹ díìsì
4

Pass through a 1280 °C zone in 10 minutes

Sinter at 1280 °C by passing the pieces through a 10 cm hot zone at 10 mm per minute: 10 minutes in the heat.

Àwọn irinṣẹ́ tí a nílò:

Ààrò Ọ̀pọ́nÀàrò Ọ̀pọ́n
Ìbọ̀wọ́ Tí Ń Fara Da OoruÌbọ̀wọ́ Tí Ń Fara Da Ooru
5

Magnetise the discs

The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.

Àwọn irinṣẹ́ tí a nílò:

Òòfà iná-mànàmánáÒòfà iná-mànàmáná
Kọ́mpasiKọ́mpasi

Àwọn ohun-èlò

3

Àwọn irinṣẹ́ tó nílò

11

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