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Lactic Acid: Fermented Whey, Lime, Oxalic Acid and Alcohol (Louradour, US Dispensatory 1907)
Whey left warm turns sour with lactic acid. Louradour's way to get the acid out: boil the whey down, take the acid up as calcium lactate with lime, then free it again with oxalic acid, which carries the lime away as an insoluble salt. A last wash in alcohol leaves the milk sugar and salts behind.
Source: The Dispensatory of the United States of America (1907), Acidum Lacticum. This is pharmacopoeial lactic acid; we use it as food-grade, as ruled. The Dispensatory gives the temperature and the order of work but no amounts or times; those are stated as not given. Vessels, filter and still are ours. Picture drawn by Youblob.
Katamtaman
1 week
Mga Tagubilin
1
1
Sour the whey at 21-27 °C
Sour the whey at 21-27 °C
Keep whey between 21.1 °C (70 °F) and 26.6 °C (80 °F) until it is charged with lactic acid. Not given: how long.
Mga materyales para sa hakbang na ito:
Tubig ng keso1 as requiredMga kailangang kasangkapan:
Sisidlang salamin
Termometrong Panlaboratoryo2
2
Boil down to a third, then add lime
Boil down to a third, then add lime
Evaporate it to one third of its bulk, decant and filter. Saturate it with milk of lime (slaked lime stirred in water). The acid becomes calcium lactate and stays dissolved; a precipitate, mostly calcium phosphate, falls. Filter again. Not given: how much lime.
Mga materyales para sa hakbang na ito:
Calcium hydroxide (apog na pinatay)1 as required
Tubig1 as requiredMga kailangang kasangkapan:
Platong Pansingaw
Pang-init na Plato
Papel na Pansala3
3
Free the acid with oxalic acid
Free the acid with oxalic acid
Add oxalic acid: the lime falls as calcium oxalate and the lactic acid is set free. Filter a third time. The solution still holds milk sugar and some salts. Oxalic acid is poisonous if swallowed: gloves. Not given: how much.
Mga materyales para sa hakbang na ito:
Asidong oksaliko dihidrato1 as requiredMga kailangang kasangkapan:
Sisidlang salaminPapel na Pansala
Gwantes na Nitrile4
4
Purify with alcohol and distil it off
Purify with alcohol and distil it off
Concentrate to a syrup and treat it with alcohol, which dissolves the acid and throws down the milk sugar and salts. Filter, then distil off the alcohol: pure lactic acid remains.
Mga kailangang kasangkapan:
Etanol - antas laboratoryo, 95 %Platong PansingawPapel na Pansala
Prasko na bilog ang ilalim
Ikid ng kondensadorPang-init na PlatoMga Materyales
4- 1 as requiredPlaceholder
- 1 as requiredPlaceholder
- 1 as requiredPlaceholder
- 1 as requiredPlaceholder
Mga Kinakailangang Kasangkapan
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