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Acrylic Pellets: Methyl Methacrylate Stirred into Beads in Gelatine Water at 75 °C (Crawford & McGrath, ICI, US 2,108,044)
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30. Ukwakira 2026DE
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Acrylic Pellets: Methyl Methacrylate Stirred into Beads in Gelatine Water at 75 °C (Crawford & McGrath, ICI, US 2,108,044)

Stirred hard enough in water with a little gelatine, methyl methacrylate breaks into droplets that harden into separate beads of acrylic instead of one solid lump. ICI's beads settle out, wash easily and go straight to the moulding press. Result: hard acrylic granules, used as moulding and extrusion pellets (they are beads, not cut pellets). Source: Crawford & McGrath, US 2,108,044 (ICI, 1938), Examples 5 and 6. Picture drawn by Youblob.
Hejuru
1 day

Amabwiriza

1

Dissolve 1 part benzoyl peroxide in 100 parts monomer

Dissolve 1 part by weight of benzoyl peroxide in 100 parts of methyl methacrylate.

Ibikoresho by'iyi ntambwe:

Metili MetakirilateMetili Metakirilate100 parts by weight
Peroxyde ya benzoylePeroxyde ya benzoyle1 part by weight

Ibikoresho bikenewe:

Umunzani w'ibiroUmunzani w'ibiro
2

Mix with 200 parts of water holding 2 parts gelatine

Mix it with 200 parts of water containing 2 parts of gelatine in solution (Example 6; Example 5 uses a soluble starch instead).

Ibikoresho bikenewe:

Ifu ya jelatineIfu ya jelatine
AmaziAmazi
Igikoresho cyo gukora polymère gifite ikotiIgikoresho cyo gukora polymère gifite ikoti
3

Stir at 1000 rpm and blow in steam to 75 °C

Stir at 1000 rpm and blow steam into the stirred mixture to bring it to 75 °C, and hold it there. After about 115 minutes the temperature starts to rise by itself: shut off the steam.

Ibikoresho bikenewe:

Igikoresho cyo kuvangaIgikoresho cyo kuvanga
Inkono itanga umwuka w'amaziInkono itanga umwuka w'amazi
Igipima Ubushyuhe cy'UbushakashatsiIgipima Ubushyuhe cy'Ubushakashatsi
4

At the 82 °C peak, cool to 60 °C with cold water

When the temperature peaks at 82 °C, cool the mixture to 60 °C by adding cold water.

Ibikoresho bikenewe:

AmaziAmazi
5

Centrifuge, wash and dry at 100 °C

Separate the granules in a centrifuge and wash them with 1 % hydrochloric acid, water, 2 % ammonia solution, and repeatedly with water. Dry them at 100 °C.

Ibikoresho bikenewe:

Santirifuje y’igisekeSantirifuje y’igiseke
Asidi ya kloridiriAsidi ya kloridiri
Umuti wa amoniyake wagabanyijweUmuti wa amoniyake wagabanyijwe
Ifuru yo kumishahoIfuru yo kumishaho

Ibikoresho

2

Ibikoresho bikenewe

11

CC0 Umurenge rusange

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