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Hydrogen Peroxide 3 %: Barium Peroxide in Dilute Sulphuric Acid
Thénard first made hydrogen peroxide from barium peroxide; the improved way stirs the peroxide into sulphuric acid, which takes the barium out as insoluble barium sulphate. Titrate the clear liquid with permanganate to find its strength, dilute it to 3 %, the mild antiseptic and bleach, and keep it in a dark bottle. Even 3 % hurts the eyes.
The picture: our diagram of the four stages.
Hejuru
A day
Amabwiriza
1
1
Peroxide into cold acid
Peroxide into cold acid
Grind the barium peroxide to a paste with a little cold water. Stand a beaker of dilute sulphuric acid in ice and stir the paste in a little at a time. Stop while a drop of the liquid still turns blue litmus red: it keeps better slightly acid.
Ibikoresho by'iyi ntambwe:
Perokside ya bariyumu150 g
Aside ya sulifuriki yoroheje1 litiroIbikoresho bikenewe:
Isekuru n'Umuhini
Umunzani w'ibiro
Igikombe cya Borosilikate
Inkono Nini
Utubuye tw'urubura
Akati k'Ikirahure ko Kuvanga
Urupapuro rwa litimusi
Amadarubindi yo Kwirinda Ibinyabutabire
Uturindantoki tw'ikawusu2
2
Filter
Filter
Let the white barium sulphate settle and filter it off. The clear liquid is hydrogen peroxide in water.
Ibikoresho bikenewe:
Akayunguruzo k'Ikirahure Gafite Umugozi
Urupapuro rwo Kuyungurura
Igikombe cya Borosilikate
Amadarubindi yo Kwirinda Ibinyabutabire
Uturindantoki tw'ikawusu3
3
Titrate a sample
Titrate a sample
Dissolve 3.161 g of permanganate to 1 litre in a volumetric flask. Pipette 1 mL of the peroxide into a flask with some dilute sulphuric acid and run permanganate in from the burette until the first lasting pink. Note the reading (step 5).
Ibikoresho bikenewe:
Perimanganate ya potasiyumu — KMnO4
Icupa ripima ubunini
Ipipete ifite ibipimo (ya Mohr)
Ikirahure cya Erlenmeyer
Bureti (y'ikirahure)
Ikibano cya laboratwari (buretti/icupa)
Aside ya sulifuriki yoroheje
Amadarubindi yo Kwirinda Ibinyabutabire
Uturindantoki tw'ikawusu4
4
Dilute and bottle
Dilute and bottle
Weigh the batch, stir in the distilled water the notebook gives, and keep it cool in a dark, closed bottle.
Ibikoresho by'iyi ntambwe:
Amazi Yatunganyijwe0.1 litiroIbikoresho bikenewe:
Umunzani w'ibiro
Akati k'Ikirahure ko Kuvanga
Icupa ry'ikirahure cy'umuhondo
Amadarubindi yo Kwirinda Ibinyabutabire
Uturindantoki tw'ikawusu5
5
Strength and dilution
Strength and dilution
Gupakira ikaye ya Jupyter…
Ibikoresho
3- Umwanya
- 1 litiroUmwanya
- 0.1 litiroUmwanya
Ibikoresho bikenewe
19- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
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