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Hydrogen Peroxide 10 %: the 3 % Solution Evaporated in Air at 75 °C, Checked with Permanganate (Thorpe 1912)
Charlie

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Charlie

30. October 2026DE
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Hydrogen Peroxide 10 %: the 3 % Solution Evaporated in Air at 75 °C, Checked with Permanganate (Thorpe 1912)

Water evaporates faster than hydrogen peroxide, so warming a weak solution in open air makes it stronger. Thorpe gives 75 °C for this first stage; we stop at 10 %, checking the strength with permanganate. Result: hydrogen peroxide of about 10 %. Source: Thorpe, Dictionary of Applied Chemistry, vol. 3 (1912), Hydrogen peroxide. Thorpe takes it on to 20 %; stopping at 10 % is ours. Danger: 10 % peroxide burns skin and eyes. Picture drawn by Youblob.
Intermediate
1 day

Instructions

1

Evaporate the 3 % solution in air at 75 °C

Warm 3 % hydrogen peroxide in an open dish at 75 °C so the water evaporates. Thorpe goes on to 20 %; ours: stop near 10 %, about a third of the starting volume. Wear goggles and gloves.

Materials for this step:

Hydrogen Peroxide (3%)Hydrogen Peroxide (3%)1 as required

Tools needed:

Evaporating DishEvaporating Dish
Water BathWater Bath
Thermometer - LabThermometer - Lab
Chemical Splash GogglesChemical Splash Goggles
Rubber GlovesRubber Gloves
2

Check the strength with permanganate

Titrate 2 c.c. in a 35 c.c. graduated tube with 5-6 drops of hydrochloric acid and a solution of 7.9 g potassium permanganate per litre until it turns red or brownish; 5 c.c. means 1 %. Ours for 10 %: dilute 1 c.c. to 2 c.c. first, so 25 c.c. means 10 %.

Tools needed:

Potassium Permanganate - KMnO₄Potassium Permanganate - KMnO₄
Hydrochloric AcidHydrochloric Acid
Distilled WaterDistilled Water
Burette (Glass)Burette (Glass)
Graduated Pipette (Mohr)Graduated Pipette (Mohr)
3

Store it cool and dark

Ours: keep the 10 % solution in a cool, dark bottle; it slowly loses strength.

Tools needed:

Amber Glass BottleAmber Glass Bottle

Materials

1

Tools Required

11

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