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Extruded Polystyrene Foam: Propylene-Blown Log Let Out at 60 °C (McIntire, Dow 1948, Ex. 3, Test 3)
Extruded polystyrene foam blown with a propylene gas fraction instead of methyl chloride. Polystyrene stands two days at 40 °C with the propylene under pressure and becomes a gel. Let out at 60 °C (300 psi in the tower), it swelled into a log 11 inches across, weighing 3.08 lb per cubic foot, with small uniform cells.
Source: O. R. McIntire (Dow), US 2,450,436 (1948), Example 3. Picture: the patent's drawing.
Osezingeni eliphezulu
3 days
Imiyalelo
1
1
Charge the tower with polystyrene
Charge the tower with polystyrene
Charge a high-pressure tower with 300 lb of granular polystyrene.
Izinto zokwakha zalesi sinyathelo:
I-Polystyrene300 lbsAmathuluzi adingekayo:
I-reactor yengcindezi
Isikali sesilinganiso
Amagilavu erabha2
2
Add the propylene fraction
Add the propylene fraction
Add 100 lb of a cracked-oil gas fraction that is about 93 % propylene, under pressure, and close the tower. Propylene is a flammable gas: no flames, strong ventilation.
Izinto zokwakha zalesi sinyathelo:
I-propylene100 lbsAmathuluzi adingekayo:
Isilinda segesi ecindezelwe
I-reactor yengcindezi
Izibuko Zokuchitheka Kwamakhemikhali3
3
Stand two days at 40 °C
Stand two days at 40 °C
Let the tower stand for two days at 40 °C while the polystyrene takes up the propylene.
Amathuluzi adingekayo:
I-reactor yengcindezi
Ithemomitha Yaselabhorethri4
4
Let it out at 60 °C
Let it out at 60 °C
Open the valved outlet near the bottom (2.5 inch in the patent) at 60 °C. The pressure is about 300 psi. The gel flows out and swells into a log 11 inches across, 3.08 lb per cubic foot, with small uniform cells. Close the outlet again. The patent heated step by step (50, 60, 75 °C) for several hours each, letting a portion out at each step.
Amathuluzi adingekayo:
I-reactor yengcindezi
Ithemomitha Yaselabhorethri
Izibuko Zokuchitheka Kwamakhemikhali
Amagilavu erabha5
5
Saw into boards
Saw into boards
When the foam has set, saw it lengthwise into slabs (ours: a woodworking saw).
Amathuluzi adingekayo:
Isaha lombazi
Amagilavu erabhaIzinto
2- 300 lbsIsibambeli
- 100 lbsIsibambeli
Amathuluzi Adingekayo
7- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
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